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51.
Meihua Hu Ning Bi Mingming Liu Shangsheng Li Taichao Su 《International Journal of Applied Ceramic Technology》2020,17(4):1629-1635
TiB2–B4C composites were in situ synthesized and consolidated by high pressure synthesis method from a mixture of TiC and B powders at the pressure and temperature of 5.0 GPa and 1500℃-1900℃. The phase composition, microstructure, density, hardness, thermal conductivity, and electrical resistivity of TiB2–B4C composites were analyzed. As the increase in the synthesis temperature, the products were TiB2 and B4C phases and that crystallinity improved. TiB2–B4C composites were dense without obvious pores. TiB2–B4C composites synthesized at 1800℃ obtained the optimized performance, including the relative density of 98.2%, the Vickers hardness of 31.7 ± 1.2 GPa with the load of 9.8 N, the thermal conductivity of 30.3 ± 0.7 W/(m K), and the electrical resistivity of 3.3 × 10−3 Ω cm, respectively. The grain size of the TiB2–B4C composites changed with the increase in synthesis temperature, leading to the changes in hardness, thermal conductivity, and electrical resistivity. 相似文献
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Libo Mei Chunming Wang Yuhang Wei Sufen Xiao Yungui Chen 《International Journal of Hydrogen Energy》2018,43(14):7102-7107
The titanium dihydride (TiH2) powder metallurgy has been attracted a lot of attention, but TiH2 powder is difficult to press moulding. In this paper, the titanium hydride powder metallurgy including TiH2 and unsaturated titanium hydrides (TiH1.5) was investigated simultaneously compared with pure titanium metal powder metallurgy. The results indicates that the titanium hydride powder metallurgy is accompanied by the deoxidation self-purification effect during dehydrogenation process for both of TiH2 and TiH1.5, which have higher sintering density than pure titanium. There are the three stages relative to densification rate, namely the slow, rapid and full densification stages for all of three materials. The compressive yield strengths increase rapidly in the rapid densification stage and are unchangeable almost in the full densification stage after holding 2 h at 1300 °C. The titanium hydride powder metallurgy is helpful to obtain much better mechanical properties than the pure titanium metal powder metallurgy. Here the compressive yield strength of the as-sintered TiH2 compact with the maximum hydrogen content is the best but has very small difference compared with that of the as-sintered TiH1.5 compact after full sintering densification. 相似文献
55.
Yan-chun ZHU Qing-xue HUANG Xiao-hui SHI Mei-rong SHUAI Wei-dong ZENG Yong-qing ZHAO Zhi-quan HUANG Li-feng MA 《中国有色金属学会会刊》2018,28(8):1521-1529
The microstructural evolution and precipitation location of the secondary phase of an as-cast Ti-25V-15Cr-0.3Si titanium alloy were investigated via isothermal compression experiments and heat treatment. The average aspect (length-to-width) ratio, average area and size of the grains at different heat treatment temperatures and holding time were analyzed and the effects of deformation and annealing time on the grain area and size were considered. It was found that the grain size was strongly influenced by the height reduction and holding time. Grain growth was significant when annealing time increased from 10 min to 2 h at 950 °C and height reduction of 30%; however, grain growth was minimal at annealing time between 2 and 4 h. Many dispersion particles were observed to form in continuous chains; the precipitation location was confirmed to be along initial grain boundaries, and the dispersion particles were identified to be Ti5Si3 phase by TEM. 相似文献
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离子膜电解工艺中,硫酸根的影响有:硫酸根易与钙离子结合,降低氯气纯度,降低电解槽电流效率。提出去除硫酸根的方法有:钡法,钙法,碳酸钡法,树脂吸附法,膜法,以及膜法+冷冻结晶法。 相似文献
59.
为探索出一种工艺简便、成本低且活菌数高的直投式纳豆菌(Bacillus natto)发酵剂的制备方法,该研究以大米粉为基质替代传统的种子液培养基培养纳豆菌后直接将其烘干制成直投式纳豆菌发酵剂,通过单因素及正交试验优化直投式纳豆菌发酵剂的制备工艺。结果表明,用含1.5%蛋白胨的大米粉作为培养基,在接种量4.0%、加水量40%、培养温度43 ℃条件下培养纳豆菌28 h,菌体生长良好,将培养物烘干后制成的直投式纳豆菌发酵剂中的活菌数含量达4.71×109 CFU/g。此技术操作简便,可推广至工业生产中,简化生产过程。 相似文献
60.
针对煤矿选煤厂直线振动筛工作过程中出现的结构故障问题,采用有限元仿真与现场测试结合的方法对振动筛出现故障的原因进行了分析研究。介绍了振动筛的主要结构及常见故障,并以某矿选煤厂发生大梁断裂的振动筛为例,对该振动筛进行三维建模和有限元模态分析,分析结果表明:随着模态阶次的增加,振型的变化逐渐由移动转为结构本身的扭曲变形。在该振动筛空载工作状态下,选用本质安全型便携式测振记录仪进行振动测试并处理测试信号,得到该振动筛的工作频率。结合模态分析结果和实际测试结果,判断出空载时频繁运行振动筛是造成其大梁断裂的主要原因。根据故障原因给出维护建议:应当尽量避免振动筛在空载或物料较少的状态下长时间运行;在振动筛投入使用前,应预先了解振动筛的工作状态及可能存在的薄弱环节,尽可能避免结构故障,保证振动筛可靠运行。 相似文献